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The near-infrared (NIR) spectral range extends from about 4000 cm to 12 500 cm between the infrared and visible regions With the exception of the R-branch of the hydrogen fluoride fundamental, the near-infrared vibrations of all common materials are overtone and combination modes, which become active as a consequence of either mechanical or electrical anharmonicity The analysis of these bands follows the same principles as those underlying the study of overtones and combination modes in the classical infrared (see Sec 23) Thus, there is no special theory of near-infrared spectroscopy Review articles on NIR spectroscopy have been published by Kaye (1954), Wheeler (1959), Goddu (1960), Whetsel (1968), and Weyer (1985) A Colthup-type chart showing the positions, the ranges, and the intensities of the absorption of characteristic functional groups has been provided by Goddu and Delker (1960).

The fact that NIR is used to a lesser extent than IR spectroscopy is partly due to the late development of appropriate instrumentation Early NIR work was performed using UV-VIS spectrometers with extension units for low wavenumbers or, vice versa, on 1R spectrometers with high wavenumber accessories The NIR spectra obtained by these methods were of low quality Instrumentational restrictions of this type no longer exist, and high-quality NIR spectra are provided by improved conventional and also by Fourier-transform (FT) spectrometers A FT-NIR atlas comprising the spectra of approximately 2000 substances in the wavenumber range 3800 to 10 500 cm has been edited (Buback and Vogele, 1993) The corresponding digital spectra are available from Chemical Concepts (Weinheim, FRG.

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Next, Ross resets the local bridge (known as MX-3510) so that it can obtain and boot from the new load image The bridges Ross uses are designed to get their boot and configuration files from a number of different servers that might exist on a network In Frame 3 15, the bridge broadcasts for a proprietary boot server; in Frame 3 16, the bridge broadcasts for a BOOTP server; in Frame 3 17, the bridge broadcasts for a DEC file server using DEC s Maintenance Operations Protocol (MOP); finally, in Frame 3 18, the bridge broadcasts a RAW Request looking for its Internet address This operation is successful and the bridge uses its IP address to broadcast a TFTP Read request (Frame 320) The SPARCstation (Maestro) responds, triggering the bridge to request a file transfer of the boot image using TFTP (Frame 327).

) The application of NIR spectroscopy has been further stimulated by the development of NIR diffuse reflectance techniques which are widely used in the analysis of agricultural, pharmaceutical, biochemical and synthetic polymer materials (Siesler, 199 1) The rapidly increasing use of NIR spectroscopy is illustrated in the book Making Light Work: Advances in Near infrared spectroscopy , edited by Murray and Cowe (1992) as well as in the Handbook of Near-Infrared Analysis by Bums and Ciurcak (1992) Considering the enormously large number of combination and overtone transitions that is calculated for polyatomic molecules, one might expect that the near-infrared spectrum consists of too many absorption components to be of any practical value for qualitative and quantitative analysis Inspection of measured NIR spectra, however, shows that even larger molecules exhibit only relatively few bands This finding is explained by a transition to local modes at higher energy (Mills, 1992).

The remarkable simplicity of NIR spectra is somewhat reduced when Fermi resonance coupling gives rise to additional absorption components (see Figs 62-8 and 62-9) The occurrence of relatively few bands.

Since ml is always an integer, then mj must have a half integer and j must be a half integer, either j l 1 or j l 1. Alternatively, for a given l value, we have two 2 2 possible values of j, j l 1 or j l 1. For example, for l 1 (p state), we have 2 2 j l 1 1 or j l 1 3. We designate these states as p1/2 and p3/2, 2 2 2 2 respectively. E.11 PARITY

Unfortunately, the file transfer is not successful (see Frame 1393) Details of the error response (Trace 1 0 2 ~indicate aTransfer Size Error, with 22 bytes ) of additional data present This error message prompts Ross to speculate that the boot image file should have been transferred in FTP Binary mode instead of ASCII mode..

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